Copper phosphotungstate catalyzed a series of aldehydes and acetic anhydride synthesis of the corresponding acetyl acetal reaction. Result shows that formaldehyde and acetic anhydride substance ratio is 1:2. Copper phosphotungstate takes amount of aldehyde accounted for only 0.5% (molar ratio) the reaction can be completed in a relatively short period of time, the product yield of 62% to 96%. The catalyst in the presence of ketones and aldehydes at the same time, can selectively react with aldehyde.
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